Technical Forum

Huaxi Special Steel Manufacturing Co., Ltd
Heat Treatment, Seamless Steel Pipe, Normalizing, Quenching, Tempering, Annealing

Heat Treatment Process of Seamless Steel Pipes

Date:2025-12-26

Seamless steel pipes are an important industrial material, and their performance directly affects their safety and service life. Heat treatment is a crucial step in improving the mechanical properties and microstructure of seamless steel pipes. The main heat treatment processes include normalizing, quenching, tempering, and annealing. The main steps and technical points of heat treatment for seamless steel pipes will be detailed below.


Preparatory Work Before Heat Treatment of Seamless Steel Pipes

1. Material Inspection

Before heat treatment, the seamless steel pipes must undergo rigorous inspection, including chemical composition analysis, dimensional measurement, and surface defect inspection, to ensure that the material meets the heat treatment requirements.


2. Cleaning Treatment

Remove oil, scale, and other impurities from the surface of the seamless steel pipes to prevent uneven heating or surface defects during heat treatment. Common methods include alkaline washing, acid washing, or mechanical cleaning.


3. Furnace Loading Preparation

Based on the steel pipe specifications and heat treatment requirements, the furnace loading method and support structure should be rationally designed to ensure uniform heating and prevent deformation.


Seamless Steel Pipe Heat Treatment


Seamless Steel Pipes Normalizing Treatment

1. Heating Stage

Heat the seamless steel pipe to 30-50°C above its critical temperature (Ac3 or Acm). Typically, this is 880-950°C for carbon steel and may be higher for alloy steel. The heating rate should be controlled at 100-150°C/h, and slower for larger pipes.


2. Holding Stage

Determine the holding time based on the seamless steel pipe's wall thickness, generally calculated at 1.5-2.5 minutes/mm, to ensure complete austenitization.


3. Cooling Stage

Allow the pipe to cool naturally in still air at a uniform rate. For steel pipes with high alloy content, the cooling rate may need to be controlled.


Seamless Steel Pipes Quenching Treatment

1. Heating Stage

Similar to normalizing, but the temperature is typically 20-30°C higher to ensure complete austenitization. Higher temperatures may be required for high-alloy steels.


2. Holding Stage

The holding time is slightly longer than normalizing to ensure sufficient dissolution of carbides and homogenization of composition.


3. Rapid Cooling

Use water, oil, or polymer solutions as the quenching medium. The cooling rate must be fast enough to suppress the pearlite transformation and obtain a martensitic structure. Care must be taken to control the uniformity of cooling to prevent deformation and cracking.


Seamless Steel Pipes Tempering Treatment

1. Heating Stage

Heat the quenched steel pipe to a temperature below Ac1 (usually 150-650), the specific temperature depending on the steel grade and performance requirements.

Item

Temperature

Functions

Low-temperature tempering

150-250

Reduces internal stress and maintains high hardness; suitable for tool steels.

Medium-temperature tempering

350-500

Improves the elastic limit; suitable for spring steels.

High-temperature tempering

500-650

Comprehensively improves strength and toughness, eliminates quenching brittleness; suitable for structural steels.


2. Holding Stage

The holding time is generally 1-2 hours; thick-walled seamless steel pipes require a longer time to ensure temperature uniformity.


3. Cooling Stage

Typically, cooling is performed in air. For steels with temper brittleness, rapid cooling through the brittle temperature range may be necessary.


Seamless Steel Pipes Annealing Treatment

1. Full Annealing

Heating to 30-50°C above Ac3, holding at that temperature, and then slowly cooling (furnace cooling) is used to refine grains and relieve stress.


2. Incomplete Annealing

Heating to between Ac and Ac is used for hypereutectoid steels to reduce network carbides.


3. Spheroidizing Annealing

Heating to near Ac1 and holding for a long time causes carbides to spheroidize, improving machinability.


4. Stress-Relief Annealing

Heating to 500-650°C, holding at that temperature, and then slowly cooling is mainly used to eliminate residual stress generated by cold working or welding.


Special Heat Treatment Processes of Seamless Steel Pipes

1. Quenching and Tempering

A combination of quenching and high-temperature tempering achieves a good balance of strength and toughness, commonly used for high-strength seamless steel pipes.


2. Solution Treatment

For seamless austenitic stainless steel tubes, heat to 1050-1150°C and rapidly cool to dissolve carbides and improve corrosion resistance.


3. Stabilization Treatment

For austenitic stainless steel containing Ti and Nb, hold at 850-930°C and then air cool to stabilize the microstructure.


Post-Heat Treatment

1. Straightening

Seamless steel pipes may deform after heat treatment and require straightening.


2. Non-destructive Testing

Including ultrasonic testing and eddy current testing to check the internal quality of the heat-treated steel tubes.


3. Performance Testing

Samples are taken for tensile, impact, and hardness tests to ensure compliance with standards.


4. Corrosion Protection

Depending on the application requirements, surface treatments such as shot peening, phosphating, or oiling may be necessary.


Seamless Steel Pipes


Key Quality Control Points of Seamless Steel Pipes

1. Temperature Control

The temperature uniformity of the heating furnace should be controlled within ±10°C, with even greater precision required during critical stages.


2. Time Control

Holding time must be sufficient but not excessive to prevent grain coarsening or decarburization.


3. Cooling Control

Cooling rate and uniformity directly affect microstructure transformation and must be strictly controlled according to steel grade.


4. Deformation Control

Ensure dimensional accuracy through proper furnace loading, support, and the use of straightening equipment.


5. Surface Protection

Prevent oxidation and decarburization by using a protective atmosphere or vacuum heat treatment.


Common Problems and Solutions

1. Insufficient Hardness

May be due to insufficient heating temperature, insufficient holding time, or excessively slow cooling rate; process parameters need adjustment.


2. Excessive Deformation

Optimize furnace loading, use specialized fixtures, and add a straightening process if necessary.


3. Cracking

Control heating and cooling rates to avoid stress concentration; special attention is needed for high-carbon steels.


4. Inhomogeneous Microstructure

Ensure uniform heating and appropriately extend holding time.


5. Surface Oxidation

Use a protective atmosphere or vacuum heat treatment, or perform subsequent pickling.


Summary

In summary, the heat treatment process for seamless steel pipes is a systematic project. It requires a scientifically formulated process plan based on the material composition, dimensions, and final application requirements, and strict control of each step to achieve the desired microstructure and properties. With technological advancements, intelligent heat treatment equipment and process simulation technology are being increasingly widely applied in the field of seamless steel pipe heat treatment.

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